Strong charge and spin fluctuations in La{}_{2}O{}_{3}Fe{}_{2}Se{}_{2}

Strong charge and spin fluctuations in LaOFeSe

Abstract

The electronic structure and magnetic properties of the strongly correlated material LaOFeSe are studied by using both the density function theory plus (DFT+) method and the DFT plus Gutzwiller (DFT+G) variational method. The ground-state magnetic structure of this material obtained with DFT+ is consistent with recent experiments, but its band gap is significantly overestimated by DFT+, even with a small Hubbard value. In contrast, the DFT+G method yields a band gap of 0.1 - 0.2 eV, in excellent agreement with experiment. Detailed analysis shows that the electronic and magnetic properties of of LaOFeSe are strongly affected by charge and spin fluctuations which are missing in the DFT+ method.

pacs:
71.20.-b, 71.27.+a, 75.30.-m,

I Introduction

Because of their close relationship with the Fe-based high-T superconductor, there has been revived interest in iron oxychalcogenides, O (=rare earth element, =transition metal element, =S or Se), which have similar crystal structures. Zhu et al. (2010); Free and Evans (2010) One example is LaOFeSe (LOFS), which was first explored by Mayer et al.,Mayer et al. (1992) and considered to be a strongly correlated material composed of the transition metal ion Fe. Analogous to its oxychalcogenides relatives, LOFS was determined to be a semiconductor by experiment and claimed to be a Mott insulator.Free and Evans (2010)

The crystal structure of LOFS, with space group I4/mmm (No.139), is shown in Fig. 1. It is composed of alternating layered units of [LaO] and [FeOSe], stacking along the -axis. The layered sheets of [LaO], formed by edge-sharing LaO tetrahedra, expand along the - plane. The [FeOSe] layers consist of face-sharing FeOSe octahedra, where the Fe atom is surrounded by two axial oxygen atoms and four equatorial selenium atoms, forming a tilted Fe-centered octahedron with the D point symmetry. Viewed along the -axis, the Fe atoms in [FeOSe] layer form checkerboard lattice, and the Fe-Fe interactions are mediated by Fe-O-Fe and Fe-Se-Fe bonds.

Despite of the considerable research in the past, there are still some mysteries about this material to be understood. First, the magnetic structure of LOFS was found to be anti-ferromagnetic(AFM) below the critical temperature T 90 K. However, two possible magnetic ground states have been proposed by experiments. The first model (Model I) was proposed in Ref. Free and Evans, 2010. Within this model, the AFM ground state is described by the propagation vector k=(0.5, 0, 0.5), and the Fe ions form a spin-frustrated magnetic structure, which align ferromagnetially along the -axis and antiferromagnetially along the -axis. Free and Evans (2010); Landsgesell et al. (2014) An interesting aspect of this magnetic structure is that it lacks inversion symmetry, which may further break the inversion symmetry of the crystal, resulting in ferroelectricity by the exchange-striction effect as possible magnetic ferroelectrics. Fiebig (2005); Cheong and Mostovoy (2007) The second model (Model II) is a non-collinear AFM model, which is composed of two magnetic sublattices with propagation vectors = (0.5, 0, 0.5) and = (0, 0.5, 0.5), respectively. This magnetic structure was first proposed by Fuwa et. al.Fuwa et al. (2010) for NdOFeSe and was identified as the magnetic structure for LOFS by recent experiments. Günther et al. (2014); McCabe et al. (2014) Within this model, the spins align in parallel in each sublattice, and perpendicular between different sublattice. In contrast with Model I, the magnetic structure of Model II still possesses the inversion symmetry.

Second, the magnitude of the local magnetic moment measured by different experiments scatters significantly, ranging from 2.62  to 3.50 . Landsgesell et al. (2014); Free and Evans (2010); Günther et al. (2014); McCabe et al. (2014) Thus information from reliable first-principles calculations will be helpful to clarify the sitution.

Third, LOFS was determined to be a semiconductor by electrical resistivity measurement, with a small band gap of 0.17-0.19 eV. Zhu et al. (2010); Lei et al. (2012); Landsgesell et al. (2014) However, the band gaps obtained by the DFT+ method, even for very small Hubbard parameters, are significantly larger than the experimental values. This suggests that the Hartree-Fock type treatment of electron correlations, which neglects the multiplet effects, might not be sufficient for this system.

Figure 1: (a). Crystal structure of LOFS, where green, red, blue and yellow balls represent La, O, Fe and Se, respectively; (b) FeOSe octahedra, where the Fe atom is surrounded by two axial oxide ions and four equatorial selenide ions, forming a tilted Fe-centered octahedron with the D point symmetry (c) Symmetry points in the Brillouin zone.

In this paper, we first identify the ground-state magnetic structure of LOFS via first-principles calculations. We calculated the total energies of different magnetic structures using density-functional theory (DFT), with on-site Coulomb interaction correction (DFT+), including the two experimentally proposed magnetic structure models. Our results suggest that Model II is the ground state-magnetic structure of LOFS. However, the DFT+ method greatly overestimates the band gap of LOFS. Zhao et al. (2013) In order to correctly describe the electronic structure of LOFS,Zhu et al. (2010); Lei et al. (2012) we further calculated the electronic and magnetic properties of this compound by the DFT plus Gutzwiller (DFT+G) method. With appropriate , , parameters, the obtained DFT+G band gap is approximately 0.1 eV - 0.2 eV, in excellent agreement with experiment. The local magnetic moment obtained by DFT+G is about 3.0 , falling within the range of experimental results, but is somewhat smaller than the DFT+ values, which are approximately 3.4 - 3.6 . Detailed analysis shows that there are strong charge and spin fluctuations in this system, which are responsible for a significant reduction of the band gap.

The rest of the paper is organized as follows. In Sec.II, the methods used in our calculations are described. In Sec. III A, we determine the ground-state magnetic structure of LOFS by comparing the total energies of various spin configurations using DFT+ method. In Sec. III B, we study its band structure using DFT+G method. A summary of our work is given in Sec: IV.

Ii Computational details

ii.1 Dft+

We perform first-principles calculations based on DFT within the spin-polarized generalized gradient approximation (SGGA) using Perdew-Burke-Ernzerhof functional, Perdew et al. (1996) implemented in the Vienna ab initio simulations package (VASP).Kresse and Hafner (1993); Kresse and Furthmüller (1996) The projector-augmented-wave (PAW) pseudopotentials with a 500 eV plane-wave cutoff are used. To account for the correlation effect of Fe ions, we add on-site Coulomb interaction as is done in the DFT+ scheme.Anisimov et al. (1991) The total energies are converged to 10 eV.

ii.2 Dft+g

LOFS is a strongly correlated system, whose band structure understandably cannot be well described by single-particle mean-field approximations like DFT+. As mentioned above and detailed below, the band gap obtained from DFT+ calculations are too big. To correct this, we resort to the DFT+G variational method,Bünemann et al. (1998); Deng et al. (2009) which can treat the multiplet effects more accurately. The DFT+G method starts with the following many-body Hamiltonian,

(1)

The first term in Eq. (1) is a - tight-binding (TB) Hamiltonian constructed from non-spin-polarized GGA band structure, projected to the - manifold of maximally localized Wannier functions. Marzari and Vanderbilt (1997); Souza et al. (2001); Marzari et al. (2012); Mostofi et al. (2008) This term apparently describes the hopping of electrons. The Wannier functions contains not only the localized 3 orbitals of Fe atoms, but also extended 2 orbitals of O atoms and 4 orbitals of Se atoms. Using the Wannier functions, the TB term can be written more explicitly as,

(2)

where the operator () creates (annihilates) a 3 electron of Fe atom on site , with orbital and spin . Likewise, () creates (annihilates) a electron of O and Se atoms.

The second term in Eq. (1) is a rotationally invariant Coulomb interaction Hamiltonian describing the strong on-site electron-electron interactions within the 3 orbitals of Fe atoms. We assume the spherical symmetry of local environment of the Fe atom and use a full interaction tensor as . For the detailed definition of the tensor, we follow the method described in Ref. Wang et al., 2015. Within the complex spherical harmonics basis, the second term of the Hamiltonian in Eq. (1) can be explicitly expressed as,Georges et al. (2013)

(3)

where the tensor satisfies the condition,

(4)

Here, , , and are the orbital index, , denote the spin states, are the Gaunt coefficients, and is the Slater integrals. For the shell, =0, 2, 4, and hence the full tensor can be specified by the parameters , and . According to Wang et. al.,Wang et al. (2015) / = 0.625 is an approximation with good accuracy for the d shell,de Groot et al. (1990) and hence is also adopted in this work. The intra-orbital Coulomb interaction and Hund’s rule coupling are set to be , and , respectively. Therefore, given the parameter values of either , or , , we can construct the full interaction U tensor.

The last term of Eq. (1) is a double-counting (DC) term in order to substrate the correlation effect which has been partially included in DFT calculations. The DC term is not uniquely defined, and here we adopted the choice used in Ref. Liechtenstein et al., 1995, where it can be expressed as

(5)

The Gutzwiller trial wave function is constructed by applying a projection operator on the uncorrelated wave function from DFT calculations,

(6)

with

(7)

where are the eigenstates of the on-site Hamiltonian for site R, and are the Gutzwiller variational parameters to be determined by minimizing the total-energy of the ground state , through the variational method.Bünemann et al. (1998); Deng et al. (2009) More details of this method can be found in Refs. Deng et al., 2009 and Lanat et al., 2012.

Iii results and discussion

In this section, we first study the magnetic ground state of LOFS using the DFT+ method. The most stable magnetic configuration coming out from our DFT+ calculations agrees with the one proposed by Fuwa and coworkers.Fuwa et al. (2010) However, as mentioned above, the DFT+ method significantly overestimates the band gap of LOFS. We then study the band structure of LOFS using the DFT+G method.

Figure 2: (a)-(g) The magnetic structures of one layer of Fe atoms in the crystalline plane. Only the Fe atoms are shown in figures, which is indicated by large blue circles; and the small red circle and yellow cross represent up and down spin orientation, respectively.

iii.1 Results from DFT+

In order to identify the magnetic structure of the ground state, we performed a series of DFT+ total energy calculations for different magnetic configurations. In LOFS, each unit cell contains two [FeOSe] layers along the -axis. Atomic positions of the second [FeOSe] layer are shifted by (0.25, 0.25, 0.25) of the lattice vectors relative to the first layer. Possible magnetic configurations in each layer are shown in Fig. 2. The magnetic structures in a unit cell are then the combinations of the magnetic configurations of the two layers. For example the configuration [(b)+(a)] means the first layer takes configuration (b), whereas the second layer takes configuration (a). This notational system is similar to that used by Zhu et. al.Zhu et al. (2010) and Zhao et. al.Zhao et al. (2013)

We calculated the total energies of seven magnetic structures, including (1) FM[(a)+(a)], (2) AFM1[(c)+(c)], (3) AFM2[(b)+(a)], (4) AFM3[(g)+(g)], (5) AFM4[(d)+(f)], (6) AFM5[(e)+(e)], (7) AFM6[(d)+(d)]. In the AFM3 configuration, the spins in each [FeOSe] layer form a double stripe AFM structure along the -axis, Free and Evans (2010), which is different from the structure used in Ref. Zhu et al., 2010 and Ref. Zhao et al., 2013. AFM3 is actually the experimental magnetic structure Model I proposed by Free et. al.,Free and Evans (2010) whereas the AFM6 configuration corresponds to the experimental magnetic model II, within the collinear approximation. Such an approximation was previously adopted for SrFFeOS in Ref. Zhao et al., 2013, because the magnetic-anisotropy energies are rather small compared to the energy differences between different configurations (see below).

Experimentally it was found that the spins form AFM along the -axis. We calculate the total energy of spin configurations with propagation vectors (1/2,0,1/2) and (1/2,0,0) for the experimental magnetic model I (AFM3, using a 212 supercell. We found that the energy difference between the AFM spin configuration along the -axis with magnetic propagation vector =(0.5, 0, 0.5), and the ferromagnetic configuration along -axis with propagation vector =(0.5, 0, 0), is only about 0.1 meV in a 212 sueprcell. Therefore, in the following studies, we ignore the anti-ferromagnetic configuration between the unit cells along the -axis, and focus on the magnetic structure in the plane. To accommodate all seven magnetic structures, we use a 221 supercell. The corresponding Monkhorst -mesh is set to 884.

The calculated energies for different magnetic configurations, are listed in Table LABEL:tab:En_vs_mag_gga for various effective Coulomb =-, where , and are the Coulomb and Hund’s exchange interactions respectively . One can see that, for all , the total energy of AFM6 is significantly lower than those of AFM3 and other spin configurations. The magnetic ground state of LOFS is then determined to be AFM6 for all the values of considered in our DFT+ calculations. We therefore conclude that the experimental magnetic structure Model II should be the ground state magnetic structure in LOFS. These results are consistent with previous DFT+ calculations for SrFFeOS. Zhao et al. (2013) We note however, in Ref. Zhu et al., 2010, the ground state of LOFS was determined to be AFM6 for =0, 1.5 and 3.0 eV, but changed to AFM1 at =4.5 eV.

FM AFM1 AFM2 AFM3 AFM4 AFM5 AFM6
0 0 159.65 15.67 -120.09 -40.61 -10.04 -128.78
1.5 0 -237.42 -52.06 -237.12 -236.51 -341.42 -394.25
3.0 0 -220.76 -49.52 -194.86 -194.88 -273.04 -303.11
4.5 0 -184.12 -42.42 -148.38 -148.49 -201.93 -219.38
Table 1: Relative energy E (meV/unit cell) of different magnetic configurations and various parameter (unit in eV), with the reference energy of FM, where the crystal structure was constrained at I4/mmm space group symmetry.

For comparison, we also calculated the total energies of different magnetic configurations for PrOFeSe, which has the similar crystal structure as LOFS.Ni et al. (2011) We found that its magnetic ground state is also AFM6 within the DFT+U approximation, the same as that of LOFS and SrFFeOS. Zhao et al. (2013) These results suggest that the Model II magnetic structure should be the common character for the oxychalcogenide materials OFeSe (=rare earth).

(eV) 0 1.5 3.0 4.5
magmom() - 3.4 3.5 3.6
Table 2: Magnetic moment (magmom) of LOFS, calculated by DFT+ method, under AFM6 magnetic configuration with different .

After determining the ground-state magnetic structure, we calculate the magnetic moments of LOFS in the AFM6 configuration for different values of . The results are listed in Table LABEL:tab:magmom_sgga_u. The calculated magnetic moments of the Fe ion for different values are around 3.4  - 3.6 , which are in agreement with the experimental result 3.50 , obtained by McCabe et. al.McCabe et al. (2014)

Figure 3: (a) Band structure of LOFS calculated by DFT+ method, under the ground state magnetic structure AFM6 and =1.5 eV. The Fermi energy have been set to 0 eV. (b) The band gap of LOFS as a function of calculated by DFT+ method, under ground state magnetic structure.

To study the electronic structure of LOFS, we calculated the band structure and density of states (DOS) by using the DFT+U method for the AFM6 spin configuration, using different Coulomb =0 – 6.0 eV. The typical band structures of LOFS with =1.5 eV are shown in Fig. 3(a). Even for a small Coulomb =1.5 eV, the band gap is as large as 1.12 eV, which is significantly larger than the energy gap 0.17 eV - 0.19 eV, extracted from the electrical resistivity measurement.Zhu et al. (2010); Lei et al. (2012) The calculated band gaps as a function of are shown in Fig. 3(b). For =0, the system is metallic. For 0, there is a nearly linear dependence of the band gap upon the value as can be seen from Fig. 3(b). For a reasonable =4.5 eV, the calculated band gap is approximately 2.0 eV, which is about one order of magnitude larger than the experimental value. The results suggest that the correlation effects are not accounted for adequately by the DFT+ method, and more advanced methods are needed to describe the electronic structure of LOFS.

Figure 4: Band structure of LOFS, calculated by DFT+G, with =6.0 eV and =0.25, under ground state magnetic structure. The Fermi energy have been set to 0 eV.

iii.2 Results from DFT+G

To correctly describe the electronic structure of LOFS, we then performed DFT+G calculations under the ground state magnetic structure AFM6. We do calculations with a series of Hubbard =3.0 - 7.0 eV and Hund’s exchange =0.1  - 0.3 . We show the results here for typical parameters =6.0 eV, =0.25 , which corresponds to =-=4.5 eV in the DFT+ calculations.

The band-structure calculated with typical =6.0 eV and =0.25  is shown in Fig. 4. The DFT+G calculated band gap is approximately 0.121 eV, which is in excellent agreement with the value obtained by the electric resistivity measurement.Zhu et al. (2010); Lei et al. (2012) This is in stark contrast with those obtained from DFT+ calculations. For example, DFT+U gives a very large band gap (approximately 2.28 eV) with =4.5 eV. These results clearly demonstrate that the multiplets effects, which are missing in the DFT+ methods but captured in the DFT+G method, are crucial for a correct description of the electronic structure of LOFS.

We also calculate the magnetic moments of Fe atoms using the Gutzwiller wave functions. The magnetic moments of Fe atoms are approximately 3.08  for =6.0 eV and =0.25 . This value is between the experimental results of Ref. Free and Evans (2010) and Ref. Günther et al. (2014), which are somehow smaller than those obtained from DFT+ calculations.

The differences between the DFT+ and DFT+G methods are that the DFT+G methods correctly take account of the multiplets effects whereas in DFT+ methods only a single atomic configuration is considered. To understand the results, we further analyzed the Gutzwiller wave functions. We calculated the probability of the atomic multiplets of Fe atoms using the Gutzwiller ground state wave function , using the relation = . To display the atomic configuration more explicitly, the crystal field splitting of Fe atom is shown in Fig. 5. The ten major atomic configurations with relatively large population are shown in Fig. 6(a), and corresponding populations are shown in Fig. 6(b) for =6.0 eV, and =0.25 .

Figure 5: Energy levels of Fe 3d states under crystal field splitting.
Figure 6: (a) Illustration of main atomic configurations with relatively large probability; (b) Probability of the atomic configurations in the Gutzwiller wave function , calculated with =6.0 eV and =0.25 , under ground state magnetic structure. Here, the atomic configurations with occupation number 5, 6, 7 and 8, are represented by histograms with color yellow, red, blue and green, respectively.

First we look at the electron occupation number of these atomic configurations. The atomic configurations cf1 has occupation number =5 (yellow), and has the population P(=5) = 0.015. Configurations cf2, cf3 have occupation number 6 (red), and their total population P(=6) = 0.247. Configurations cf4, cf5, cf6, cf7, cf8 have occupation number 7 (blue) and total population P(=7) = 0.4438, and configurations cf9, cf10 have occupation number 8 (green) with total population P(=8) = 0.0826. These results suggest that there are strong charge fluctuations on the Fe ions. Although the local interaction in this material is quite strong leading to Mott insulator behavior, the charge and spin fluctuation is still strong for such a multi-orbital system, which reduces the single particle gap from the value obtained by Hatree-Fock-type approximation (i.e. DFT+) to about 0.1-0.2 eV.

Besides the charge fluctuation, there are also strong spin fluctuation on the Fe atoms. Configurations cf3, cf8, cf9, cf10 have total spin =2. The total population of these configurations is P(=2) = 0.0827. Configurations cf4, cf5, cf6, cf7 have total spin =3, and the their total population is P(=3) = 0.4438. Configuration cf2 has =4, and P(=4) = 0.247, and cf1 has =5 with P(=5) = 0.015. The most populated spin states in DFT+G calculations are =3, which is smaller than the formal magnetic state =4 in DFT+ calculations. As a result, the DFT+G calculated magnetic moments of Fe ions are smaller than those calculated by DFT+ methods.

Iv Summary

We have studied the electronic structure and magnetic properties of the strongly-correlated material LaOFeSe, using both DFT+ and DFT+G methods. The ground states magnetic configuration obtained from DFT+ calculations are in agreement with most recent experiments.McCabe et al. (2014); Günther et al. (2014) However, DFT+ calculations greatly overestimate the band gap of the material. We then investigate electronic structure using the DFT+G method, and the results show LaOFeSe is a narrow gap semiconductor, in excellent agreement with experiments. We show there are strong charge and spin fluctuations on the Fe atoms that greatly reduce the band gap and magnetic moments from the DFT+ values.

Acknowledgements.
LH acknowledges the support from Chinese National Science Foundation Grant number 11374275.

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